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The attachment states that some brass did not change in hardness over time like a straight horizontal red line but other brass did. Could this be brass like Lapua uses?
I anneal after every firing. I'm still using the original cases I bought 2 years ago (Lapua), when I switched to 6mm dasher. I anneal the neck and 1/4" below the shoulder. Cycle time for these cases is about 10+with no problems and good seating tension. I'm using the "GinaErick" induction annealing machine so the annealing is precise and consistent.
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Correct,college kids that are educated by engineers and professors ,not everyone that reloads has studied metallurgy ...probably why the OP asked the question in the first place .I wonder if you may be misunderstanding the link you provided. "Over time" is not months and years at room temperature. In this instance, it is the time the samples were heated in an oven and in this instance it is measured in minutes at a high temperature.
And it was not different kinds of brass involved in this test. The experiment was measuring the change in hardness for the identical samples which differed only in the amount of cold working they had undergone prior to going into the oven. Remember, we're talking temperatures of 400C. The samples which were significantly work hardene were harder to begin with and they became softer the longer they were in the oven. The samples with less work hardening were softer to begin with and they changed the least during the time they were in the oven. This is not rocket surgery.
And yes, this is very close to the kind of brass Lapua and all other cartridge makers use. Recipes vary to some degree with trace amounts of other metals and not every brand uses the exact same brass, but basically the brass we shooters use is 70/30 cartridge brass and it can all be expected to react like the samples used in the link you provided.
None of this is news to those who have studied metallurgy. The effects mentioned in the link are well understood. These kinds of experiments are the sort of things college students do.
I think this may depend on the amount the brass has been worked to cause work hardening.
If the brass has not been worked much a larger grain size can be obtained after annealing. If the brass has been extensively cold worked the grain size reduction or hardness reduction will not be as great as with brass that has not been cold worked as much.
To achieve this bushing dies or dies that have a honed neck area like Forster F/L dies will help combined with neck turning. The objective is to have necks expand the minimum amount after firing yet permit a slip fit after firing and have adequate neck tension to hold the bullet. Common ordinary dies excessively work necks to provide a "one size fits all" solution for reloading, like hold the bullet regardless of neck wall thickness.
All this involves measurements of chamber, neck walls, and fired cases.
I guess annealing after 3 firings combined with carefully sized brass neck to chamber fits would work.
I don't know about F/L sizing and annealing. It appears that annealing would have little effect on head space and the work hardness of the cartridge head or base would need to be preserved and kept cool during the annealing process, like don't cook the whole case in some oven.
http://che.uri.edu/course/che333/Annealing of 70-30 Brass.pdf
The attachment states that some brass did not change in hardness over time like a straight horizontal red line but other brass did. Could this be brass like Lapua uses?